Jb. Yang et al., PREPARATION OF (GAMMA-STATE HOT-PRESSING(ALPHA(2)) TYPE TIAL INTERMETALLICS FROM ELEMENTAL POWDERS BY SOLID), Materials science and technology, 13(8), 1997, pp. 695-701
A hot isostatic pressing (hipping) process is often employed to prepar
e dense TiAl based intermetallics by liquid phase sintering in the ele
mental powder metallurgy (EPM) field. However; hot pressing which is c
heaper than hipping, not only in preparation but also in operation, is
seldom used in this field since it results in the aluminium melting a
nd overflowing during sintering. In the present work, the solid state
hot pressing process has been developed to prepare TiAl intermetallics
from elemental powders by a continuous two stage sintering cycle incl
uding a solid state diffusion stage and a densification stage. The eff
ect of process variables such as temperature, pressure, and time on th
e density and microstructure of specimens was investigated. The result
s showed that dense (alpha(2) + y) type TiAl intermetallics can be obt
ained after sintering at 630 degrees C for 22 h (with the first 5 h at
45 MPa), followed by 2 h at 1250 degrees C and 45 MPa. (C) 1997 The I
nstitute of Materials.