M. Grivet et al., ELECTRON-MICROSCOPY ANALYSIS OF KRYPTON ION TRACKS INDUCED IN DURANGOAPATITE, Nuclear tracks & radiation measurements, 22(1-4), 1993, pp. 779-782
The, track annealing phenomenon, which occurs in a heated mineral cont
aining uranium like apatite, is analysed using the transmitted electro
n microscopy (TEM) associated to the platinium shadowed carbon replica
method. The diameters of 86Kr (1,66 MeV/nucleon) ion tracks induced n
ormally to the observation plane are measured during an etching stage
with a very low concentrated etchant (HNO3 1%). The distribution of tr
ack diameters in a sample, and its variation following the annealing a
mount the apatite knew, lead us to agree with the track registration m
odel which let appear more than one microscopic defect structure (Dart
yge et al., 1981). This model cannot be observed with only unannealed
etched tracks, but is clearly highlighted by the thermal annealing of
nuclear tracks in this mineral. The opening track profile is analysed
as a determination of the etching speed variation versus the distance
to the ion trajectory. The variation is shown to be dependent on the c
ristallogaphy of the apatite. The different etching speeds, relative t
o the orientation with the c-axis of the apatite, influence the track
shape for long etching times. The etched pit figure is not symetrical,
and present in the c-axis direction a much more width opening than th
e etched track diameter. Finaly, the lateral track shape and the etche
d pit are supposed to be sensitive to the etchant strength.