Sorghum undergoes structural changes during tempering, steam cooking,
and flaking at various tempering moisture levels. Physical properties
of flakes, digestibility, birefringence, scanning electron microscopy
(SEM), and environmental SEM (ESEM) were used to evaluate the quality
of steam-flaked sorghum from grain containing 11-23% water. As moistur
e levels increased, the flakes became stronger (57-69% whole flakes) a
nd less dusty (9-4% fines). The diameter of the flakes varied among mo
isture levels, but preflake and final flake moisture contents increase
d as the temper level increased. Starch birefringence remained unchang
ed after tempering, and decreased only slightly after steam cooking; g
elatinization occurred primarily during the flaking process. The steam
ing process prepared the grain for flaking by heating and softening th
e kernels. Tempering allowed extra water to penetrate inside the kerne
l endosperm. More starch granules had the opportunity to reach the gla
ss transition temperature (T-g) during flaking. Based on subjective ev
aluation, birefringence, and SEM, poor quality flakes were opaque, cha
lky in appearance, and prone to high levels of breakage. The starch gr
anules were more intact and less tightly packed into the flake. Good q
ualify flakes were translucent, thin, and strong, with little chalkine
ss, and low levels of dust and fines. The dehydrated gelatinized starc
h continuous phase surrounding the granules reduced the amount of air
spaces within the flake, increasing the translucency. ESEM inspection
revealed that starch was more extensively gelatinized in the tempered
samples. The starch granules were much larger in diameter, and the rel
ative level of gelatinization, evident by the presence of starch granu
les with collapsed centers, was much higher.