M. Egami et Y. Shiohara, GROWTH SHAPE-ANALYSIS OF ROUND YBA2CU3O7-X SINGLE-CRYSTAL FABRICATED BY THE PULLING METHOD, Physica. C, Superconductivity, 282, 1997, pp. 463-464
We constructed an automatic crystal pulling system for YBa2Cu3O7-x(Y12
3) and made a round cornered single crystal by keeping its growth temp
erature around its peritectic temperature. The size of the round shape
crystal was 4 mm in diameter and 4 mm in length[1]. A seed crystal wa
s remelted at its corner first, and after the rounded cornered crystal
was grown. Along the vertical axis, the crystal corner became wavy. T
he remelting process was explained by free energy difference between t
he flat interface to the square one. Growth shapes of the round corner
were explained by temperature dependent growth rate anisotropy.