HYDROGEN-ATOMS LOCATION IN [RE-4(MU(3)-H)(4)(CO)(12)] BY JOINT X-RAY SINGLE-CRYSTAL AND NEUTRON POWDER DIFFRACTION ANALYSIS

Authors
MASCIOCCHI N DALFONSO G KOCKELMANN W SCHAFER W SIRONI A
Citation
N. Masciocchi et al., HYDROGEN-ATOMS LOCATION IN [RE-4(MU(3)-H)(4)(CO)(12)] BY JOINT X-RAY SINGLE-CRYSTAL AND NEUTRON POWDER DIFFRACTION ANALYSIS, Chemical communications, (19), 1997, pp. 1903-1904
Citations number
23
Categorie Soggetti
Chemistry
Journal title
Chemical communications → ACNP
ISSN journal
13597345
Issue
19
Year of publication
1997
Pages
1903 - 1904
Database
ISI
SICI code
1359-7345(1997):19<1903:HLI[BJ>2.0.ZU;2-9
Abstract
The hydrogen atom locations in [Re-4(mu(3)-H)(4)(CO)(12)] are accurate ly determined by joint X-ray single-crystal and time-of-flight neutron powder diffraction analysis; this new methodology does not require la rge crystals of several mm dimensions but only a sizeable amount of mo nophasic microcrystalline sample.