Jh. Edgar et al., HARDNESS, ELASTIC-MODULUS AND STRUCTURE OF INDIUM NITRIDE THIN-FILMS ON ALN-NUCLEATED SAPPHIRE SUBSTRATES, Journal of materials science. Materials in electronics, 8(5), 1997, pp. 307-312
The structural properties of epitaxial indium nitride thin films were
characterized and related to the mechanical properties as measured by
nanoindentation. The seven epitaxial InN films examined were deposited
over the temperature range 200-400 degrees C by reactive magnetron sp
uttering on (00.1) sapphire substrates buffered with a thin AlN layer.
The hardness, surface texture and crystal quality of the InN films we
re functions of the deposition temperature, with the maximum hardness
(11.2 GPa), the smoothest surface, the minimum c-lattice constant (0.5
708 nm), and the minimum (00.4) X-ray rocking curve width (0.6 degrees
) all occurring at the deposition temperature of 350 degrees C. The cr
ystal quality and the hardness of the InN films degraded at both highe
r and lower temperatures.