AN AC CALORIMETER PROBE FOR A CLOSED-CYCLE CRYOGENIC STATION

Citation
Jf. Jurado et al., AN AC CALORIMETER PROBE FOR A CLOSED-CYCLE CRYOGENIC STATION, Measurement science & technology, 8(10), 1997, pp. 1151-1155
Citations number
9
Categorie Soggetti
Instument & Instrumentation",Engineering
ISSN journal
09570233
Volume
8
Issue
10
Year of publication
1997
Pages
1151 - 1155
Database
ISI
SICI code
0957-0233(1997)8:10<1151:AACPFA>2.0.ZU;2-S
Abstract
The AC temperature technique is used to develop a calorimeter probe fo r measuring the specific heat of small samples. A commercial closed-cy cle refrigerator operating in the 8-300 K temperature range was used a s a cryogenic station. A theory of operation is presented and the expe rimental set-up is discussed. The calorimeter has been used to study t he nature of the magnetic and order-disorder phase transitions of seve ral materials. Specific heat data taken from a sample of chromel alloy (90% Ni-10% Cr) and a single-crystal sample of RbAS(4)I(5) show that the sensitivity of the apparatus to relative variations in the specifi c heat is about 0.1%.