E. Kendi et al., -1,2,3,4,5,6,7,8-OCTAHYDROQUINAZOLINE-2,5-DIONE(I) AND ENYL)-1,2,3,4,5,6,7,8-OCTAHYDROQUINAZOLINE-2,5(II), Crystal research and technology, 32(6), 1997, pp. 857-863
The crystal and molecular structures of the title compounds have been
determined by x-ray structure analysis. The compounds (I) and (II) cry
stallize in space groups P2(1)2(1)2(1) and I2/a respectively. The stru
ctures were solved by direct methods and refined to R = 0.058 and R =
0.046. The saturated pyrimidine-2-one ring in both structures deviates
from the planarity. There are two intermolecular hydrogen bonds in (I
) and (II). The configuration at C4 in (I) is S.