I. Samajdar et al., TEXTURAL CHANGES THROUGH GRAIN-GROWTH IN TI-BEARING IF-STEEL INVESTIGATED BY ORIENTATION IMAGING MICROSCOPY AND X-RAY-DIFFRACTION, ISIJ international, 37(10), 1997, pp. 1010-1015
Textural changes were investigated using X-ray diffraction and orienta
tion imaging microscopy (OIM). During normal grain growth, slight incr
ease in gamma-fibre (ND//[111]) was observed. Prolonged annealing and
a resultant[rant abnormal grain growth, however, decreased gamma and i
ncreased ct (RD//[110]). The decrease/increase in fibres were mainly c
aused by corresponding changes in F [{111}[112]] and l [{112}[110]] or
ientations, while E [{111}[110]] and H [{001}[110]] components did not
change significantly. OIM characterization of grain boundary nature i
ndicated an approximate increase in the fraction of low angle (<20 deg
rees) boundaries with increasing annealing time;At the initiation of a
bnormal grain growth, the fraction of low angle boundaries (specially
those with 1-5 degrees misorientation) were observed to have reached a
relatively large value. Such observations may fit well with a simple
scheme: the transient strengthening in gamma-fibre was possibly caused
by normal grain growth of;l-grains. Al the later stages of grain grow
th, the growth of the gamma-grains was possibly inhibited/stopped by g
rains of similar orientations. This, in turn, may increase the fractio
n of low angle boundaries. When the fraction of low-angle/low-mobility
boundaries reached a critical value, growth of certain grains (as F/E
in our case) were inhibited/pinned, while few of the more favourable
placed/oriented grains could grow abnormally. Measured values of 'free
length', defined as the average distance between an i (where i may be
F/E/I/H) and al (where j is less than 20 degrees misoriented with i)
grain, showed the highest value for [ and the lowest for F. Free lengt
h can be considered as an average distance for non-interrupted growth.
Highest free length Values for I, caused by the spatial locations, po
ssibly favored abnormal grain growth of i grains.