Mj. Duer, DETERMINATION OF STRUCTURAL DATA FROM MULTIPLE-QUANTUM MAGIC-ANGLE-SPINNING NMR EXPERIMENTS, Chemical physics letters, 277(1-3), 1997, pp. 167-174
It has recently been shown that multiple-quantum magic-angle spinning
(MQMAS) NMR spectroscopy produces high-resolution spectra for half-int
eger quadrupolar nuclei which suffer second-order quadrupole coupling.
The present work shows how the effects of magnified dipole-dipole cou
pling in MQMAS spectra can be analysed to produce quantitative structu
ral data. (C) 1997 Elsevier Science B.V.