SYNTHESIS AND STRUCTURAL CHARACTERIZATION OF AN S-LINKED CALIX[3]AZINE

Citation
M. Mascal et al., SYNTHESIS AND STRUCTURAL CHARACTERIZATION OF AN S-LINKED CALIX[3]AZINE, Tetrahedron letters, 38(43), 1997, pp. 7639-7640
Citations number
9
Categorie Soggetti
Chemistry Inorganic & Nuclear
Journal title
ISSN journal
00404039
Volume
38
Issue
43
Year of publication
1997
Pages
7639 - 7640
Database
ISI
SICI code
0040-4039(1997)38:43<7639:SASCOA>2.0.ZU;2-G
Abstract
An S-linked, heterocyclic calix[3]arene analogue 2 is prepared by cond ensation of a dichloro-1,3,5-triazine with sulfide ion. X-ray structur al analysis shows that 2 is approximately disk shaped in the solid sta te, while molecular modelling indicates a high degree of conformationa l mobility. (C) 1997 Elsevier Science Ltd.