Mp. Deboer et al., INVESTIGATION OF A NEW FRACTURE-MECHANICS SPECIMEN FOR THIN-FILM ADHESION MEASUREMENT, Journal of materials research, 12(10), 1997, pp. 2673-2685
We have investigated mechanical probing of a precracked fine line stru
cture as a new type of thin film fracture mechanics specimen. An ideal
ized mechanics analysis is first presented. Experimentally, two types
of precracks are formed. A thin carbon layer to which other layers wea
kly adhere creates a ''processed precrack'' by integrated circuit proc
essing techniques. An ''indented processed precrack'' is formed by pre
cision alignment of a sharp microwedge. The processed precrack is foun
d to reduce the critical tangential load by 50% from a non-precracked
Line, while the indented processed precrack lowers the load by 200%. F
rom this, a reasonable value of adhesion may be directly calculated. C
rack path behavior is observed to depend on strength of the interface.
In the case of a weak interface, the crack remains in the interface a
s it extends. For a strong interface, it kinks into the substrate if t
he crack is initially short, but remains in the interface if it is ini
tially long. Given the experimental evidence, the mechanics are slight
ly modified to quantitatively model the experimental data.