Two methods for the determination of total mercury content in environm
ental samples, soils and sediments, were compared. Dissolution procedu
re of soils, sediments, and biological material under elevated pressur
e followed by determination of mercury by cold vapour atomic absorptio
n spectrometry using a MHS-1 system and direct total mercury determina
tion without any chemical pretreatment from solid samples using a Trac
e Mercury Analyzer TMA-254 were compared. TMA-254 was also applied for
the determination of mercury in various further standard reference ma
terials. Good agreement with certified values of environmental referen
ce materials was obtained.