Jw. Arnold et al., THE DISINTEGRATION OF SUPEREBA CEMENT IN SOLUTIONS WITH ADJUSTED PH AND OSMOLARITY, Journal of endodontics, 23(11), 1997, pp. 663-668
This study determined the disintegration of fast-set SuperEBA cement u
sing ANSI/ADA Specification No. 30 (Spec #30) as well as modifications
in pH, osmolarity, time before immersion, and duration of immersion t
hat mimic the clinical, endodontic application of this material. After
immersion intervals of 24 h, 1 wk, 1 m, 3 m, or 6 m, specimens were d
esiccated and weighed. The preimmersion and postdehydration weights we
re obtained to the nearest 1.0 mg and the percent weight loss from pre
immersion levels was calculated. Adjusting the osmolarity to the physi
ologic level of 300 mOsm/kg resulted in significantly less weight loss
(p < 0.05) than the control group in distilled water (no modification
of Spec #30). The pH of the storage solution was found to be a signif
icant factor in weight loss. As the acidity and the time of immersion
increased, the weight loss also significantly increased with the great
est weight loss of 19.81% at pH 5.5 after 6 m storage. Immersion withi
n 10 min of mixing was not significantly different (p > 0.05) in weigh
t from the control of 1 h set-time. The 24 h weight loss measurements
for the pHs of 5.5 and 6.4 were greater than the 1.5% allowed by Spec
#30. All other 24 h measurements were less than the 1.5%.