A LINE-SHAPE ANALYSIS FOR SPIN-1 NMR SIGNALS

Authors
DULYA C ADAMS D ADEVA B ARIK E ARVIDSON A BADELEK B BALLINTIJN MK BARDIN D BARDIN G BAUM G BERGLUND P BETEV L BIRD IG BIRSA R BJORKHOLM P BONNER BE DEBOTTON N BOUTEMEUR M BRADAMANTE F BRESSAN A BULTMANN S BURTIN E CAVATA C CRABB D CRANSHAW J CUHADAR T DALLATORRE S VANDANTZIG R DERRO B DESHPANDE A DHAWAN S DYRING A EICHBLATT S FAIVRE JC FASCHING D FEINSTEIN F FERNANDEZ C FROIS B GALLAS A GARZON JA GAUSSIRAN T GEHRING R GIORGI M VONGOELER E GOERTZ S GOMEZ F GRACIA G DEGROOT N PERDEKAMP MG GULMEZ E HARMSEN J VONHARRACH D HASEGAWA T HAUTLE P HAYASHI N HEUSCH CA HORIKAWA N HUGHES VW IGO G ISHIMOTO S IWATA T KABUSS EM KAGEYA T KALINOVSKAYA L KAREV A KESSLER HJ KETEL TJ KISHI A KISSELEV Y KLOSTERMANN L KRAMER D KRIVOKHIJINE V KROGER W KUKHTIN V KUREK K KYYNARAINEN J LAMANNA M LANDGRAF U LEGOFF JM LEHAR F DELESQUEN A LICHTENSTADT J LINDQVIST T LITMAATH M LOWE M MAGNON A MALLOT GK MARIE F MARTIN A MARTINO J MATSUDA T MAYES B MCCARTHY JS MEDVED K MEYER W VANMIDDELKOOP G MILLER D MORI K MOROMISATO J NAGAITSEV A NASSALSKI J NAUMANN L NIINIKOSKI TO OBERSKI JEJ OGAWA A OZBEN C PARKS DP PERROTKUNNE F PESHEKHONOV D PIEGAIA R PINSKY L PLATCHKOV S PLO M POSE D POSTMA H PRETZ J PUSSIEUX T PYRLIK J REICHERZ G REYHANCAN I RIJLLART A ROBERTS JB ROCK S RODRIGUEZ M RONDIO E ROSADO A SABO I SABORIDO J SANDACZ A SAVIN I SCHIAVON P SCHULER KP SEGEL R SEITZ R SEMERTZIDIS Y SEVER F SHANAHAN P SICHTERMANN EP SIMEONI F SMIRNOV GI STAUDE A STEINMETZ A STIEGLER U STUHRMANN H SZLEPER M TEICHERT KM TESSAROTTO F TLACZALA W TRIPET A UNEL G VELASCO M VOGT J VOSS R WEINSTEIN R WHITTEN C WINDMOLDERS R WILLUMEIT R WISLICKI W WITZMANN A YANEZ A YLOSTALO J ZANETTI AM ZAREMBA K ZHAO J
Citation
C. Dulya et al., A LINE-SHAPE ANALYSIS FOR SPIN-1 NMR SIGNALS, Nuclear instruments & methods in physics research. Section A, Accelerators, spectrometers, detectors and associated equipment, 398(2-3), 1997, pp. 109-125
Citations number
21
Categorie Soggetti
Nuclear Sciences & Tecnology","Physics, Particles & Fields","Instument & Instrumentation",Spectroscopy
Journal title
Nuclear instruments & methods in physics research. Section A, Accelerators, spectrometers, detectors and associated equipment → ACNP
ISSN journal
01689002
Volume
398
Issue
2-3
Year of publication
1997
Pages
109 - 125
Database
ISI
SICI code
0168-9002(1997)398:2-3<109:ALAFSN>2.0.ZU;2-0
Abstract
An analytic model of the deuteron absorption function has been develop ed and is compared to experimental NMR signals of deuterated butanol o btained at the SMC experiment in order to determine the deuteron polar ization. The absorption function model includes dipolar broadening and a frequency-dependent treatment of the intensity factors. The high-pr ecision TE signal data available are used to adjust the model for Q-me ter distortions and dispersion effects. Once the Q-meter adjustment is made, the enhanced polarizations determined by the asymmetry and TE-c alibration methods compare well within the accuracy of each method. In analyzing the NMR signals, the quadrupolar coupling constants could b e determined for both the C-D and the O-D bonds of deuterated butanol.