AMBIENT PERTURBATION REDUCTION IN MICROSIZED CALORIMETRIC SYSTEMS

Citation
J. Lerchner et al., AMBIENT PERTURBATION REDUCTION IN MICROSIZED CALORIMETRIC SYSTEMS, Thermochimica acta, 302(1-2), 1997, pp. 201-210
Citations number
8
Categorie Soggetti
Chemistry Analytical
Journal title
ISSN journal
00406031
Volume
302
Issue
1-2
Year of publication
1997
Pages
201 - 210
Database
ISI
SICI code
0040-6031(1997)302:1-2<201:APRIMC>2.0.ZU;2-O
Abstract
To avoid thermostatting effort in a calorimeter the influence of ambie nt temperature perturbations on the output signal can be reduced by pr edicting and correcting the perturbation part of the output signal of the calorimeter. The prediction can be verified by measuring the tempe rature perturbations and simulating the corresponding output signal. U sing a dynamical model of the calorimeter, simple methods for the solu tion of this problem are shown and tested experimentally. (C) 1997 Els evier Science B.V.