SYNTHESIS AND MESOMORPHIC PROPERTIES OF SOME 3,6-DISUBSTITUTED CYCLOHEX-2-ENONES

Citation
V. Bezborodov et al., SYNTHESIS AND MESOMORPHIC PROPERTIES OF SOME 3,6-DISUBSTITUTED CYCLOHEX-2-ENONES, Molecular crystals and liquid crystals science and technology. Section A, Molecular crystals and liquid crystals, 303, 1997, pp. 297-304
Citations number
29
Categorie Soggetti
Crystallography
ISSN journal
1058725X
Volume
303
Year of publication
1997
Pages
297 - 304
Database
ISI
SICI code
1058-725X(1997)303:<297:SAMPOS>2.0.ZU;2-V
Abstract
The synthesis and mesomorphic properties of several dozen 3,6-disubsti tuted cyclohex-2-enones are described. The compounds were obtained by the condensation of 4-substituted beta-(N,N-dimethylamino)ethylphenyl ketone hydrochlorides (Mannich salts) with 2-alkylacetoacetic esters. The influence of the structure of the reactants, catalysts and solvent s on the yield is discussed.