R. Colombo et S. Tiraferri, METHOD OF COLUMN EXTRACTION FOR COUMAPHOS RESIDUE DETERMINATION IN HONEY, Industrie alimentari, 36(363), 1997, pp. 1151-1153
A simple method of column extraction for Coumaphos (active principle u
sed against varroasis affecting honeybees) residue determination in ho
ney is presented. Extraction involves sample dispersion on diatomaceou
s earth (Extrelut) and a subsequent eluition by Dichloromethane. Recov
ery trials gave satisfactory results. Compared to traditional liquid-l
iquid fractioning, the method offers significant advantages such as sm
aller consumption of organic solvents, glassware, and of time.