Js. Vetrano et al., INFLUENCE OF THE PARTICLE-SIZE ON RECRYSTALLIZATION AND GRAIN-GROWTH IN AL-MG-X ALLOYS, Materials science & engineering. A, Structural materials: properties, microstructure and processing, 238(1), 1997, pp. 101-107
Recrystallization and grain growth studies of Al-Mg-X (where X is Mn,
Zr or Sc) alloys have been carried out using a combination of optical
and transmission electron microscopy of interrupted heating tests, cha
nges in hardness, and in-situ observations in the transmission electro
n microscope. Nucleation sites have been identified as typically large
(> 1 mu m diameter) eutectic constituent particles, but also occasion
ally clusters of sub-micron dispersoids. By altering the density and s
ize of the Mn-, Sc- and Zr-based particles with selected thermomechani
cal treatments, recrystallization could be suppressed up to temperatur
es near the melting point. These results can be explained by examinati
on of the stored energy from cold work and the particle-substructure i
nteractions due to the precipitate morphology. Implications of these r
esults for grain size control in Al-Mg based alloys will be discussed.
(C) 1997 Elsevier Science S.A.