APPLICATION OF TRIFLUOROACETIC-ANHYDRIDE SODIUM-IODIDE REAGENT FOR SELECTIVE DETECTION IN THIN-LAYER CHROMATOGRAPHY .4. THIN-LAYER CHROMATOGRAPHIC DIFFERENTIATION OF NITRONES, NITROXIDE RADICALS AND NITROSOAMINES IN MIXTURES
A. Kotynski et Zh. Kudzin, APPLICATION OF TRIFLUOROACETIC-ANHYDRIDE SODIUM-IODIDE REAGENT FOR SELECTIVE DETECTION IN THIN-LAYER CHROMATOGRAPHY .4. THIN-LAYER CHROMATOGRAPHIC DIFFERENTIATION OF NITRONES, NITROXIDE RADICALS AND NITROSOAMINES IN MIXTURES, Journal of chromatography, 663(1), 1994, pp. 127-131
Trifluoroacetic anhydride-sodium iodide mixture (TFAA-I) reacts with n
itroxide radicals, nitrones and nitrosoamines with release of iodine.
Methods for the differentiation of these groups of nitrogen derivative
s containing the N-O moiety using TLC systems with TFAA-I detection re
agent are described.