A combination treatment (dry-heat and glucoamylase) was applied on pot
ato starch granules. Many inner granules in the granules after the tre
atments were observed by SEM. The inner granule located near edge of e
llipsoid of granule was partially degraded X-ray diffraction pattern o
f starch granules did not change before and after the treatments in sp
ite of over 50% loss by amylase digestion. GPC and iodine reaction of
the sample showed the treatments brought about fairly large degradatio
n of both amylopectin and amylose components, but GPC of debranched sa
mple after the combination treatments showed amylose was thoroughly de
graded while peaks pattern of amylopectin did not change. Small size g
ranules were more susceptible than large size granules by the treatmen
ts.