A variety of trace analytical methods (solid-phase and liquid-liquid e
xtraction, HPLC and GC-MS) for quantitatively assessing the input and
behavior of pesticides and their metabolites (i.e., triazines, acetami
des, phenoxy acids and organotin compounds) in natural waters and sedi
ments are presented. The results of field studies illustrate the analy
tical methods performance such as simultaneous determination of compou
nds with different polarities, low detection limits, and high precisio
n and accuracy.