Nanostructured M50 type steel materials were prepared by hot pressing
the precursor powders. The precursor powders were chemically synthesiz
ed using Mo different techniques, namely, thermal decomposition and co
-reduction. During the hot press process, the precursor powders were t
ransformed to nanocrystalline phases with the precipitation of fine ca
rbides. Simultaneously, the crystalline powders were densified. The de
nsified samples were studied using both conventional and high resoluti
on transmission electron microscopy. The effects of hot pressing param
eters such as temperature, time and pressure on the development of nan
ostructures, grain growth and formation of defects are discussed.