J. Karthikeyan et al., NANOMATERIAL POWDERS AND DEPOSITS PREPARED BY FLAME SPRAY PROCESSING OF LIQUID PRECURSORS, Nanostructured materials, 8(1), 1997, pp. 61-74
Ultrafine grained Al2O3, Mn2O3, ZrO2 and Y2O3-ZrO2 powders and deposit
s were produced by flame spray processing of atomized precursor soluti
ons. Ceramic particles of 1-150 nm size were collected on an electrost
atic precipitator at a rate of similar to 5-20 mg/min, with similar to
5-25% collection efficiency. Nanograined oxide deposits with a powder
morphology were produced at a deposition efficiency of < 10%. The spr
ay feedstock and processing conditions affected the size, shape and ph
ase composition of the synthesized nanomaterials. Particles with wider
distributions of larger size grains were produced from aqueous soluti
ons, whereas narrow range of fine-grained material was produced from o
rgano-metallic precursors. Liquid flame spraying is a viable technique
to produce nanoparticles and deposits.