COMPARISON OF A STYRENE-DIVINYLBENZENE COPOLYMERIC ANION-EXCHANGER AND A POLYMETHACRYLATE COPOLYMERIC ANION-EXCHANGER FOR GLUCOSINOLATE SEPARATION

Citation
C. Elfakir et al., COMPARISON OF A STYRENE-DIVINYLBENZENE COPOLYMERIC ANION-EXCHANGER AND A POLYMETHACRYLATE COPOLYMERIC ANION-EXCHANGER FOR GLUCOSINOLATE SEPARATION, Journal of liquid chromatography & related technologies, 20(6), 1997, pp. 907-921
Citations number
15
Categorie Soggetti
Chemistry Analytical","Biochemical Research Methods
ISSN journal
10826076
Volume
20
Issue
6
Year of publication
1997
Pages
907 - 921
Database
ISI
SICI code
1082-6076(1997)20:6<907:COASCA>2.0.ZU;2-W
Abstract
Studies on gradient elution were undertaken on a Hamilton PRP-X100 col umn. Satisfactory analysis was produced by using a concentration gradi ent in which the eluent ion concentration was increased over the run. To conclude the overall investigation of glucosinolate separation by a nion exchange chromatography, a polymethacrylate copolymeric anion exc hanger was evaluated and compared with a silica anion exchanger and a polystyrene-divinylbenzene copolymeric anion exchanger for an isocrati c analysis of glucosinolates. Different commonly used inorganic and or ganic anions as well as alkanesulfonate anions and borate-gluconate mi xtures were tested as aqueous mobile phase.