L. Decaro et al., EFFECTS OF THE ELASTIC STRESS-RELAXATION ON THE HRTEM IMAGE-CONTRAST OF STRAINED HETEROSTRUCTURES, Acta crystallographica. Section A, Foundations of crystallography, 53, 1997, pp. 168-174
In this work, the effects of the elastic relaxation of compositional s
tresses caused by the finite size of transmission electron microscopy
(TEM) specimens on the image contrast of high-resolution transmission
electron microscopy (HRTEM) micrographs of strained heterostructures m
ade by cubic materials are investigated. The reduced spatial dimension
s, owing to the thinning process of strained heterostructures, cause m
odification of the atomic positions in the thinned specimens with resp
ect to the bulk ones. This deformation is a function not only of the s
pecimen thickness but also of the thinning crystallographic direction.
The results show that the strains of an elastically relaxed structure
can vary by 15% as a function of the thinning direction ([100] or [01
1]). The bending of the atomic columns caused by the elastic relaxatio
n phenomena in HRTEM specimens of strained semiconductor materials can
cause a strong background-intensity variation in the HRTEM images. Th
is effect is a function of the structure of the investigated materials
, indicating that information on the background intensity variation, o
wing to the non-uniform lattice distortion of an elastically relaxed h
eterostructure made by cubic materials, is contained in the {200} beam
s. Thus, the influence of the elastic relaxation cannot be neglected w
henever HRTEM is used to deduce the local chemical composition or the
local unit cell in strained cubic materials.