A VERSATILE NMR TECHNIQUE FOR THE IDENTIFICATION OF PHOSPHORYLATION SITES IN OLIGOSACCHARIDES

Authors
SCHRAML J DEBRUYN A CONTRERAS R HERDEWIJN P
Citation
J. Schraml et al., A VERSATILE NMR TECHNIQUE FOR THE IDENTIFICATION OF PHOSPHORYLATION SITES IN OLIGOSACCHARIDES, Journal of carbohydrate chemistry, 16(2), 1997, pp. 165-170
Citations number
6
Categorie Soggetti
Chemistry Inorganic & Nuclear",Biology
Journal title
Journal of carbohydrate chemistry → ACNP
ISSN journal
07328303
Volume
16
Issue
2
Year of publication
1997
Pages
165 - 170
Database
ISI
SICI code
0732-8303(1997)16:2<165:AVNTFT>2.0.ZU;2-4
Abstract
A combination of two well-established NMR methods, namely, phosphorus decoupling and 1D-TOCSY, provides identification of phosphorylation si tes in a simple and straightforward manner in small to medium-sized ol igosaccharides. The method is demonstrated on Man-P-GlcMan(7)GlcNAc(2) , a glycoprotein-derived N-linked type oligosaccharide.