Y-1-METHYL-3-PHENYL-1,2,3,4-TETRAHYDROISOQUINOLINE

Authors
PIZARRO JL ARRIORTUA MI TELLITU I BADIA D DOMINGUEZ E OCHANDO L AMIGO JM DEBAERDEMAEKER T
Citation
Jl. Pizarro et al., Y-1-METHYL-3-PHENYL-1,2,3,4-TETRAHYDROISOQUINOLINE, Acta crystallographica. Section C, Crystal structure communications, 53, 1997, pp. 355-358
Citations number
15
Categorie Soggetti
Crystallography
Journal title
Acta crystallographica. Section C, Crystal structure communications → ACNP
ISSN journal
01082701
Volume
53
Year of publication
1997
Part
3
Pages
355 - 358
Database
ISI
SICI code
0108-2701(1997)53:<355:Y>2.0.ZU;2-Z
Abstract
Ambiguous information obtained from H-1 NMR spectroscopy has prompted an investigation of the correct stereochemistry of the title compound, C34H39NO3Si, by X-ray diffraction analysis. An uncommon pseudoaxial-a xial trans conformation was observed for the substituents Linked to th e C-4 and C-3 atoms (IUPAC numbering). The pseudo-equatorial conformat ion of the methyl group joined to the C-l atom was also confirmed.