DEVELOPMENT OF THE SIMULTANEOUS THERMAL-ANALYSIS X-RAY-SCATTERING MEASUREMENT SYSTEM

Authors
YOSHIDA H KINOSHITA R TERAMOTO Y
Citation
H. Yoshida et al., DEVELOPMENT OF THE SIMULTANEOUS THERMAL-ANALYSIS X-RAY-SCATTERING MEASUREMENT SYSTEM, Thermochimica acta, 264, 1995, pp. 173-183
Citations number
17
Categorie Soggetti
Chemistry Analytical
Journal title
Thermochimica acta → ACNP
ISSN journal
00406031
Volume
264
Year of publication
1995
Pages
173 - 183
Database
ISI
SICI code
0040-6031(1995)264:<173:DOTSTX>2.0.ZU;2-B
Abstract
A new simultaneous DSC/X-ray measurement system was developed for the purpose of combining X-ray scattering data and calorimetric data. The DSC/X-ray measurement system was equipped with a conventional wide-ang le X-ray diffractometer (WAXD). The phase transition behavior of pure hexatriacontane was measured by the DSC/WAXD, both on heating and cool ing. The accuracy and reproducibility of the simultaneous DSC/X-ray in strument were comparable with the conventional DSC.