M. Prazak et S. Holecek, TEMPERATURE OSCILLATIONS IN EUTECTIC ALLOY MELT FOR THE BRIDGMAN-STOCKBARGER CONFIGURATION, Crystal research and technology, 30(7), 1995, pp. 933-941
The characteristics of the temperature field in AlZn, AlGe, PbSn, and
Sb-InSb low-melting alloy eutectics were determined by means of the Br
idgman-Stockbarger method of directional solidification with a specime
n fixed in a graphite ampoule and a moving furnace. The device could b
e rotated in such a way, that an arbitrary angle alpha between the axi
al temperature gradient in the melt and the gravity field vector could
be set. Periodic and/or nonperiodic temperature fluctuations indicati
ng periodic and/or nonperiodic turbulent convection up to an angle alp
ha = 80 degrees were studied in the individual systems. At larger angl
es laminar convection can be expected. The frequency of the temperatur
e oscillations is the same along the entire length of the specimen, wh
ilst the amplitudes of the temperature oscillations depend on the situ
ation of the measurement in the specimen. It has been found that the z
one of unstable periodic convection is reduced with an increase of the
axial temperature gradient and a decrease of the H/d ratio for a cyli
ndrical ampoule. The convection instability threshold in the ampoule i
ncreases with the deviation of the ampoule axis from the axis of the v
ertical unstable arrangement, i.e. from the direction of the gravity v
ector. The threshold of the laminar now instability and the onset of t
urbulent flow increases with the H/d ratio, i.e. an ampoule with a hig
her H/d ratio stabilizes laminar flow.