SYNTHESIS OF DEUTERIUM-LABELED POLYOCTYLALKANES

Authors
BOLTON R LUFF S SUTCLIFFE LH
Citation
R. Bolton et al., SYNTHESIS OF DEUTERIUM-LABELED POLYOCTYLALKANES, Journal of labelled compounds & radiopharmaceuticals, 36(12), 1995, pp. 1205-1213
Citations number
18
Categorie Soggetti
Chemistry Analytical","Pharmacology & Pharmacy","Biochemical Research Methods
Journal title
Journal of labelled compounds & radiopharmaceuticals → ACNP
ISSN journal
03624803
Volume
36
Issue
12
Year of publication
1995
Pages
1205 - 1213
Database
ISI
SICI code
0362-4803(1995)36:12<1205:SODP>2.0.ZU;2-6
Abstract
The synthesis of specifically labelled 9-d-9-octylheptadecane (1) and 9-d-9,10-dioctyloctadecane (2) has been achieved using selective and s pecific deuterium labelling methods. The precursor to the latter compo und, tetraoctyl ethene, has been achieved by a variant of the McMurry reaction which improves upon recently published methods.