Hj. Scheibe et al., INVESTIGATION OF SURFACE-TOPOGRAPHY, MORPHOLOGY AND STRUCTURE OF AMORPHOUS-CARBON FILMS BY AFM AND TEM, Fresenius' journal of analytical chemistry, 353(5-8), 1995, pp. 690-694
Morphology and structure of amorphous carbon films deposited with a pu
lsed are source (LASER-ARC) have been studied using microscopical meth
ods (SEM, TEM and AFM), electron diffraction and spectro-scopical inve
stigation (EELS). The parameters of the are source and the deposition
conditions (substrate temperature) influence morphology and structure
of deposited amorphous carbon films. Especially the incorporation and
growth of particles, embedded in the film have been investigated. By p
article analysis using an optical microscope a majority of particles t
hat is smaller than 500 nm has been determined. The morphology has bee
n also demonstrated similar by AFM and TEM images. Their number and si
ze of particles is strongly influenced by the deposition temperature.
The structure of amorphous film is characterized by the EELS-spectra,
but the particle structure was not detectable.