E. Illekova et al., PECULIARITIES OF THE CRYSTALLIZATION KINETICS OF FE73.5CU1NB3SI13.5B9RIBBON TO THE NANOSTRUCTURED PHASE, Journal of non-crystalline solids, 193, 1995, pp. 556-560
Continuous heating as well as isothermal differential scanning calorim
etry was used to study the transformation of Fe73.5Cu1Nb3Si13.5B9 ribb
ons to a crystalline state. The scanning 'crystallization' peak was sm
all and wide, with a long high-temperature tail. It shifted to higher
temperatures after pre-annealing. The isothermal transformation signal
s always decreased monotonically, only the amplitude changing with tem
perature, but not the position. All of these abnormal characteristics
may be explained in terms of a grain-growth mechanism, involving the c
oarsening of already existing crystal nuclei to give the crystalline m
aterial.