This paper discusses two potential ultrasonic techniques for character
ization of fibre-matrix interphases in composites: measurements of wav
e scattering (attenuation) and its phase velocity. The implementation
procedures of these two methods are described using analytical or nume
rical models with an emphasis on their applicability. Examples of ultr
asonic characterization of interphases are given for ceramic and inter
metallic matrix composites reinforced with large diameter SIC fibres.
Carbon-rich interphase coatings are added on these fibres to improve c
omposite performance and chemical and thermal compatibility. The exper
imentally measured interphase moduli from ultrasonic data are compared
with those determined from interphase microstructures showing good ag
reement. Finally, several applications of these techniques for interph
asial damage assessment are demonstrated, including characterization o
f oxidation damage in ceramic matrix composites and of fatigue damage
in metal matrix composites. These experimental results show that ultra
sonic wave attenuation and velocity are significantly affected by degr
adation of the elastic properties of the interphasial layer; thus, bot
h methods are very useful for non-destructive assessment of interphasi
al damage.