Sd. Conzone et al., FRACTURE-TOUGHNESS OF TIB2 AND B4C USING THE SINGLE-EDGE PRECRACKED BEAM, INDENTATION STRENGTH, CHEVRON-NOTCHED BEAM, AND INDENTATION STRENGTH METHODS, Journal of the American Ceramic Society, 78(8), 1995, pp. 2187-2192
The mode I fracture toughness (K-Ic) of boron carbide (B4C) and titani
um diboride (TIB2) was determined using four competing techniques. The
indentation strength (IS), chevron notched beam (CNB), and indentatio
n fracture (IF) methods are common techniques that were compared to th
e recently standardized single-edge precrack beam (SEPB) method. The S
EPB method was more difficult to apply, but it represents the most rig
orous method for K-Ic determination, because it uses few assumptions a
nd requires a direct measurement of crack length. The IS method was an
expeditious and economical alternative when low indentation loads wer
e used. CNB K-Ic values were virtually rate-independent when displacem
ent rates less than or equal to 0.5 mm/min were used. The IF method wa
s the least satisfactory technique, because of high variability in K-c
values and because of the low differentiation between the two materia
ls studied.