Polymeric phase domains in monolayers of a styrene functionalized surf
actant are revealed by scanning force microscopy (SFM) inspection. The
monomeric films are formed and polymerized by UV irradiation at the n
itrogen-water interface and subsequently deposited on glass slides. SF
M images have features similar to fluorescence microscope images but r
eveal more details of the polymeric phase texture. Polymeric domains a
re characterized by larger thickness and different roughness. Small po
lymeric clusters are also revealed.