Rv. Krishnarao et Yr. Mahajan, EFFECT OF ACID TREATMENT ON THE FORMATION OF SIC WHISKERS FROM RAW RICE HUSKS, Journal of the European Ceramic Society, 15(12), 1995, pp. 1229-1234
Raw rice husks have been treated by boiling for I h in 5 N hydrochlori
c acid. The washed and dried acid-treated raw rice husks (TRRH) and un
treated raw rice husks (RRH) were directly pyrolysed (without precokin
g) in argon atmosphere at different temperatures between 1050 and 1600
degrees C. Silica obtained from TRRH has a lower level of impurities
than that obtained from RRH. Acid treatment has been found to decrease
the degree of crystallization of silica and carbon in rice husks. The
whisker formation has been decreased in TRRH. As the carbon loss due
to the formation of CO was high, the SiC content in the pyrolysed TRRH
was higher than that in pyrolysed RRH.