TRIETHYLAMINE POLY(HYDROGEN FLUORIDES) IN THE SYNTHESIS OF A FLUORINATED NUCLEOSIDE GLYCON

Authors
CHOU TS BECKE LM OTOOLE JC CARR MA PARKER BE
Citation
Ts. Chou et al., TRIETHYLAMINE POLY(HYDROGEN FLUORIDES) IN THE SYNTHESIS OF A FLUORINATED NUCLEOSIDE GLYCON, Tetrahedron letters, 37(1), 1996, pp. 17-20
Citations number
12
Categorie Soggetti
Chemistry Inorganic & Nuclear
Journal title
Tetrahedron letters → ACNP
ISSN journal
00404039
Volume
37
Issue
1
Year of publication
1996
Pages
17 - 20
Database
ISI
SICI code
0040-4039(1996)37:1<17:TPFITS>2.0.ZU;2-J
Abstract
The stereospecific synthesis of 6 via a highly selective, noncorrosive fluorination of 4 with Et(3)N . 3HF was discovered. The intermediate fluorosulfonate 5 was isolated, purified and its structure verified.