Nb/Fe multilayers with a Pd top layer were prepared by electron beam e
vaporation on Si substrates. The multilayer stacks were charged with h
ydrogen from the gas phase at 200 degrees C and at a gas pressure of 0
.1 mbar. The resulting hydrogen concentration profiles were measured b
y the N-15 nuclear reaction method. We find that the multilayers take
up hydrogen under these conditions, that hydrogen also reaches the low
lying layers and that hydrogen is accumulated in Nb, leaving the Fe l
ayers essentially hydrogen-free. The present work was undertaken as a
preparatory study for the investigation of the magnetic coupling of th
e Fe layers through the Nb spacers as a function of the hydrogen conte
nt.