N. Gao et al., CRACK-GROWTH MORPHOLOGY AND MICROSTRUCTURAL CHANGES IN 316-STAINLESS-STEEL UNDER CREEP-FATIGUE CYCLING, Fatigue & fracture of engineering materials & structures, 18(12), 1995, pp. 1407-1421
A study into microstructural effects and crack growth behaviour of AIS
I type 316 stainless steel under creep-fatigue conditions at 550 degre
es C within the high strain ranges of 0.9-2.5%, including a 60 min hol
d time, was undertaken on a high-temperature reverse-bending rig. Thro
ughout the tests, surface cracks on both the tensile-hold and the comp
ressive-hold sides were monitored by means of a plastic-strip replicat
ion technique. Additional investigations were conducted on failed spec
imens to examine the crack morphology in the depth direction, and to e
xamine the function of oxidation; also to study changes of fracture su
rface morphology, changes in dislocation structures and precipitate co
nfigurations corresponding to the different strain ranges. These detai
led analyses revealed that the predominantly intergranular long cracks
on the tensile-hold side and transgranular short cracks on the compre
ssive-hold side are dominant aspects of the investigation. The disloca
tion structures under creep-fatigue conditions are strain-range depend
ent, with a clearly defined cell structure at the higher strain ranges
and dense dislocation tangles at lower strain ranges. The large reduc
tion in creep-fatigue endurance can be attributed to early crack growt
h and grain boundary cracking caused by stress relaxation, oxidation,
precipitation and, most importantly, the coalescence of the many minor
surface short cracks.