A. Guelzim et al., STRUCTURE OF DIETHYL METHOXYETHOXY)-CALIX[4]ARENE-25,27-BIS(OXYACETATE), Acta crystallographica. Section C, Crystal structure communications, 49, 1993, pp. 2121-2124
We present here the synthesis and X-ray crystal structure of a new 2 2' modified p-tert-butylcalix[4]arene, diethyl utyl-26,28-bis-(2-meth
oxyethoxy)pentacyclo[19.3.1. 1(3,7). 19(26),-21,23-dodecaene-25,27-diy
ldioxy}diacetate, bearing glycol methyl ether and ethyl ester function
al groups. H-1 NMR spectra of this compound indicated that it has a co
ne conformation; this is confirmed by the crystallographic study.