DETERMINATION OF CO-60 IN ENVIRONMENTAL WATER SAMPLES BY A HYDROUS MAGNESIUM-OXIDE FILTER

Authors
Citation
Jm. Lo et Jd. Lee, DETERMINATION OF CO-60 IN ENVIRONMENTAL WATER SAMPLES BY A HYDROUS MAGNESIUM-OXIDE FILTER, Analytica chimica acta, 318(3), 1996, pp. 391-394
Citations number
7
Categorie Soggetti
Chemistry Analytical
Journal title
ISSN journal
00032670
Volume
318
Issue
3
Year of publication
1996
Pages
391 - 394
Database
ISI
SICI code
0003-2670(1996)318:3<391:DOCIEW>2.0.ZU;2-G
Abstract
Preconcentration of trace Co-60 and analogous radionuclides by adsorpt ion on MgO for their determination in environmental water samples exem plified by seawater was demonstrated. An adsorption filter fabricated by coating hydrous MgO onto a round piece of a densely twilled nylon c loth was used to facilitate separation of the radionuclides adsorbed. The MgO adsorption filter was sealed in a polyethylene column. The wat er sample analyzed was pumped through the column where the radionuclid es could be efficiently adsorbed onto the filter. Thereafter the radio nuclides enriched filter was transferred to a high-purity germanium de tector connected with a multichannel analyzer for gamma-spectrometry. The novel preconcentration technique proves to be fast and efficacious and detection of Co-60 becomes highly sensitive because of the very l arge enrichment factor.