Starch transformations, occuring in white pan bread during its baking
and shelf life up to 180 days, are studied using infrared spectroscopy
, differential scanning calorimetry (DSC), amylolysis, swelling and so
lubility measurements, compression testing and X-ray diffractometry. A
fter baking, starch in bread is greatly modified. Starch granules are
partially disrupted. Crystalline organization, characteristic of nativ
e starch, is no longer detected. Presence of minor crystalline fractio
ns is explained by the comparison of baking conditions with critical t
emperatures of phase transitions, as determined by DSC. During shelf l
ife of bread, main events occur during the first two months. After thi
s period, bread stays in a steady state. Water loss and firming of bre
ad are concomitant with starch gelation.