INTERLABORATORY CALIBRATION OF PEROXYACETYL NITRATE LIQUID STANDARDS

Citation
T. Krognes et al., INTERLABORATORY CALIBRATION OF PEROXYACETYL NITRATE LIQUID STANDARDS, Atmospheric environment, 30(6), 1996, pp. 991-996
Citations number
15
Categorie Soggetti
Environmental Sciences","Metereology & Atmospheric Sciences
Journal title
ISSN journal
13522310
Volume
30
Issue
6
Year of publication
1996
Pages
991 - 996
Database
ISI
SICI code
1352-2310(1996)30:6<991:ICOPNL>2.0.ZU;2-J
Abstract
Peroxyacetyl nitrate (PAN) solutions in the concentration range 10-100 mu g PAN per mi solvent were distributed and analyzed by ten European laboratories. Overall precision accounting for standards' preparation , transport, storage and analysis resulted in standard deviations of 1 6 +/- 8% of the mean for the high- and 25 +/- 8% for the low-end of th e concentration range. Following alkaline PAN hydrolysis, nitrite anio ns were determined, mostly by chemically suppressed ion chromatography , with better precision than the acetate anions.