Sj. Duray et al., LASER ACOUSTIC-EMISSION THERMAL TECHNIQUE (LAETT) - A TECHNIQUE FOR GENERATING ACOUSTIC-EMISSION IN DENTAL COMPOSITES, Dental materials, 12(1), 1996, pp. 13-18
Objectives. This study was designed to investigate a new method for ge
nerating interfacial debonding between the resin matrix and filler par
ticles of dental composites. Methods. A pilot study was conducted to e
valuate laser-induced acoustic emission in dental resins filled with v
arying quantities of particles. Model systems of 50/50 BisGMA/TEGDMA r
esin reinforced with 0, 25, and 75 wt% 5-10 mu m silanated BaSiO6 were
analyzed. The sample size was 3.5 mm diameter x 0.25-0.28 mm thick. A
continuous wave CO2 laser (Synrad Infrared Gas Laser Model 48-1) was
used to heat the composite samples. Acoustic events were detected, rec
orded, and processed by a model 4610 Smart Acoustic Monitor (SAM) with
a 1220A preamp (Physical Acoustic Corp.) as a function of laser power
. Results. Initially, the acoustic signal from the model composites pr
oduced a burst pattern characteristic of fracturing, about 3.7 watts l
aser power. Acoustic emission increased with laser power up to about 6
watts. At laser powers above 6 watts, the acoustic emission remained
constant. The amount of acoustic emission followed the trend: unfilled
resin > composite with 25 wt% BaSiO6 > composite with 75 wt% BaSiO6.
Significance. Acoustic emission generated by laser thermal heating Is
dependent on the weight percent of filler particles in the composite a
nd the amount of laser power. For this reason, laser thermal acoustic
emission might be useful as a nondestructive form of analysis of denta
l composites.