M. Muller et al., DISLOCATION DENSITY AND LONG-RANGE INTERNAL-STRESSES IN HEAVILY COLD-WORKED CU MEASURED BY X-RAY-LINE BROADENING, Zeitschrift fur Metallkunde, 86(12), 1995, pp. 827-831
A well proven method of high resolution X-ray line profile analysis is
applied to large-strain straight rolled samples of polycrystalline co
pper. Both the obtained dislocation densities and long-range internal
stresses show a monotonous increase within the strain stage IV, and th
en a levelling off in stage V. The local stresses of cell walls and ce
ll interiors are found to increase within stage IV even in relation to
the macroscopic stress. Together with the measured values of volume f
raction of cell walls, the strengthening in stage IV turns out to aris
e mainly from the cell interior, although it is clearly related to the
increase of total dislocation density and not so much to dislocation
rearrangements which enhance the stress field.