The design of a titanium-zirconium clamped cylinder-piston type pressu
re cell for neutron diffraction investigations under hydrostatic press
ure up to 10 kbars without supports is described. It is the first time
that Freon-11 has been used as a hydrostatic pressure transmitting me
dium. The following results carried out at the room temperature are pr
esented: the discovery of the transition from I to III phase in a LiKS
O4 single crystal and the results of the investigation on the influenc
e of pressure upon the structure of the YBaCuO HTSC obtained by means
of the powder diffraction method.