5-TERT-BUTYLTHIAZOLIDINE-2-THIONE AND 5-PHENYLTHIAZOLIDINE-2-THIONE

Authors
LAKNIFLI A PIERROT M CHANON F CHANON M
Citation
A. Laknifli et al., 5-TERT-BUTYLTHIAZOLIDINE-2-THIONE AND 5-PHENYLTHIAZOLIDINE-2-THIONE, Acta crystallographica. Section C, Crystal structure communications, 52, 1996, pp. 215-218
Citations number
10
Categorie Soggetti
Crystallography
Journal title
Acta crystallographica. Section C, Crystal structure communications → ACNP
ISSN journal
01082701
Volume
52
Year of publication
1996
Part
1
Pages
215 - 218
Database
ISI
SICI code
0108-2701(1996)52:<215:5A5>2.0.ZU;2-Y
Abstract
In the title compounds, C7H13NS2, (I), and C9H9NS2, (II), the heterocy cle adopts a half-chair conformation with a torsion angle tau = S1-C5- C4-N3 equal to 27.5(4)degrees in (I) and 30.0(3)degrees in (II). In bo th crystals, a hydrogen bond between the thione group and the N atom i s observed, the corresponding S2 ... N3 distance being equal to 3.367 (8) Angstrom in (I) and 3.376(9) Angstrom in (II).