A SINGLE-CRYSTAL X-RAY DIFFRACTOMETER FOR WHITE SYNCHROTRON-RADIATIONWITH SOLID-STATE DETECTORS - ENERGY-DISPERSIVE LAUE (EDL) INSTRUMENT AT HASYLAB, HAMBURG GERMANY
Kf. Fischer et al., A SINGLE-CRYSTAL X-RAY DIFFRACTOMETER FOR WHITE SYNCHROTRON-RADIATIONWITH SOLID-STATE DETECTORS - ENERGY-DISPERSIVE LAUE (EDL) INSTRUMENT AT HASYLAB, HAMBURG GERMANY, Nuclear instruments & methods in physics research. Section A, Accelerators, spectrometers, detectors and associated equipment, 369(1), 1996, pp. 306-311
A new instrument for X-ray diffraction offers the use of ''white'' syn
chrotron radiation on a small sample producing a Laue pattern and sele
cting parts of the spectrum for sending reflections into two energy di
spersive detectors. Integrated Bragg intensities of up to 20 ''harmoni
cs'' are obtained simultaneously. The sample is mounted on a Kappa gon
iometer with a lot of angular space around it for controlling special
environments. Possibilities are provided for energy dependent polariza
tion monitoring, for fine adjustment of the diffractometer, and for in
stalling different monochromators and auxiliary equipment for limiting
unwanted fluorescence and other background. The EDL diffractometer is
controlled via CAMAC by a PC which also handles collecting as well as
reduction of data. A number of applications are mentioned and partly
demonstrated by test results.