Gj. Foran et al., GRAZING-INCIDENCE X-RAY-DIFFRACTION STUDIES OF THIN-FILMS USING AN IMAGING PLATE DETECTION SYSTEM, Langmuir, 12(3), 1996, pp. 774-777
First results of the grazing incidence X-ray diffraction patterns of c
admium arachidate Langmuir-Blodgett (LB) films measured using imaging
plate detection are presented and discussed. The use of imaging plates
has made possible the observation of diffraction peaks at far higher
values of wavevector transfer than have been observed previously with
other methods of detection, with a dramatic increase in signal-to-nois
e ratio. Values of in-plane d-spacing, area per molecule, and position
al correlation length of the hexatic-B phase of a monolayer of cadmium
arachidate are in excellent agreement with previous measurements. Mul
tilayer LB films showed, in addition to the in-plane spots Q(110) and
Q(200), sets of off-plane diffraction spots (Q(hkl), l > 0) which are
observed up to a Q(2) value of 3.3 Angstrom(-1). Spots with both odd a
nd even values of l are observed.